Temperature in situ XRD test device
1. Product features
1) The device has good sealing performance and can perform electrochemical in-situ XRD test under temperature control conditions and XRD test under different atmospheres;
2) Simple operation, unique quick disassembly design, easy mold installation, good test consistency, to avoid the experimental deviation caused by different operation techniques;
3) The device design is flexible, good scalability, can be improved according to user requirements for temperature range and cooling rate improvement;
4) Window can be customized according to user needs (metal, non-metal X-ray window)
5) Multi-channel gas mixing system can be selected to expand gas leak detection, gas monitoring and other copy devices to achieve multi-technology.
2. Technical parameters
1) The device is composed of: high and low temperature thermostat, upper computer software, high and low temperature sample table, cavity, vacuum system, etc.
2) The high temperature heating unit uses imported resistance wire for direct heating, temperature control range from room temperature to 600.0℃(temperature can be customized, long-term operation), temperature control accuracy of ±0.1℃
3 The temperature sensor is placed on the lower side of the sample, which can truly feedback the temperature of the sample area:
4 Device dimensions 100*80 *55 mm;
5 The device adopts arc window structure, and the window material is polymer amorphous film with a thickness of 10-20 μm. Under the condition of X-ray transmission rate >95% under the condition of X-ray transmission Angle 10-90°, the traditional X-ray intensity will not be lost due to Angle.
6 The device is equipped with a conversion control table and can be used with a diffractometer or tested on synchrotron radiation